HTK GR - Cuptor cu cameră, izolație din grafit

The Graphite Furnace HTK GR operates with rough/fine vacuum, protective gases such as Nitrogen/Argon, and reactive gases like Hydrogen and Carbon Monoxide. The Graphite Furnace HTK GR cannot operate in an Oxygen atmosphere due to the Graphite insulation.

The rectangular design with a front door allows for easy loading and unloading. The HTK GR range is available in up to six different sizes. The smallest designs with a capacity of 8 litres and 25 litres are typically employed by laboratories for research and development. The 80 litre, 220 litre, 400 litre or 600 litre furnaces are predominantly used as pilot manufacturing systems or large scale production.

The HTK GR is based on Graphite insulation material, as well as graphite heating elements. With maximum temperatures up to 2200 °C, the HTK GR is suited for extreme heat treatment needs. Upon request, the system can be equipped with a Graphite retort that is capable of a defined gas guiding flow within the unit and improves temperature uniformity to < ± 10 °C. For processes with strong outgassing, the retort protects the heating elements and increases the lifetime of the furnace.

Semi-automatic Furnace HTK 8 GR 22

Video Produs: HTK GR - Cuptor cu cameră, izolație din grafit

Exemple de Aplicații

Graphitization , Pyrolysis, Siliconizare, Sinterizare, Ceramică Tehnică

Caracteristici standard

  • Graphite furnace, offering the highest possible temperatures
  • Hydrogen partial pressure operation if requested
  • Precisely controlled vacuum pumping speeds appropriate for powders
  • Data recording for quality management

HTK GR - Cuptor cu cameră, izolație din grafit Vedere în interiorul cuptorului cu grafit HTK

  1. Frame
  2. Water cooled vessel
  3. Heating cassette
  4. Groove for the sealing
  5. Front door
  6. Graphite insulation
Inside the chamber, heating elements are positioned at the bottom, left, right, and top sides of the furnace chamber allowing for improved temperature uniformity. For larger volumes, the back wall and front are equipped with heating elements to maintain excellent temperature uniformity. The HTK W, HTK MO, HTK GR and HTK KE furnaces are surrounded by a water cooled vessel; thus classifying, the HTK systems as a cold wall furnace. The cooling water is guided through the double walled vessel.

Upon request, the HTK GR can be operated up to 3000 °C. For operation at 3000 °C, the furnace is specially designed with a specific isolation thickness, optimal positioning of the heating elements, and a pyrometer for temperature measurement and control. The pyrometer directly measures the heat radiation by optical methods via a window inside the furnace and is not directly inserted into the furnace.

This measurement principle only works if a sufficient amount of radiation is emitted. The needed radiation is only generated at temperatures exceeding 400 °C. For lower temperatures, a sliding thermocouple is used to control the lower temperatures.

Because of the increasing vapor pressure of graphite, 3000 °C operation is only possible under inert gas atmosphere. Additionally, the high vapor pressure also results in carbon being released to the atmosphere. For carbon sensitive samples, a metallic high temperature furnace must be used.

View inside HTK GR

HTK GR - Cuptor cu cameră, izolație din grafit Exemple

HTK 8 GR/22-1G smart up to 2200°C

HTK 25 GR/22-1G automat până la 2200°C cu sistem opțional de piroliză 

HTK 400 GR/22-1G automatic up to 2200°C

HTK GR - Cuptor cu cameră, izolație din grafit Date tehnice

Insulation material Dimensiuni: Externe H x W x D (mm) Transport weight (kg) Usable space Volum (l) H x W x D, usable space without retort (mm) H x W x D, usable space with retort (mm) Thermal values Tmax vacuum (°C) Tmax atmospheric pressure (°C) -Delta-T, between 500 and 1500°C (K) according to DIN 17052 Max. heat-up rate (K/min) Cooling time (h) Connecting values Putere (kW) Voltage (V) Current (A) Series fuse (A) Vacuum (option) Leakage rate - clean, cold and empty (mbar l/s) Vacuum range depending on the pumping unit Cooling water required Flow (l/min) Max. inlet temperature (°C) Gas supply Nitrogen or Argon flow, others on request (l/h) Controller
HTK 8 GR/22-1G Graphite 2100 x 1300 x 1100 1200
8 200 x 200 x 200 180 x 180 x 200
2200 2200 ± 10 10 6
26.5 400 (3P) 3 x 66 3 x 80
5x10-3 rough or fine vacuum
40 23
200-2000 on request
HTK 25 GR/22-1 Graphite 2200 x 1900 x 1800 1700
25 250 x 250 x 400 230 x 230 x 400
2200 2200 ± 10 10 6
60 400 (3P) 3 x 90 3 x 125
5x10-3 rough or fine vacuum
70 23
200-2000 on request
HTK 80 GR/22-1G Graphite 2300 x 2100 x 2200 2000
80 400 x 400 x 500 380 x 380 x 400
2200 2200 ± 10 10 8
100 400 (3P) 3 x 150 3 x 200
5x10-3 rough or fine vacuum
100 23
200-2000 on request
HTK 220 GR/22-1G Graphite 2500 x 2300 x 2600 3000
220 600 x 600 x 600 560 x 560 x 560
2200 2200 ± 10 10 8
160 400 (3P) 3 x 240 3 x 315
5x10-3 rough or fine vacuum
150 23
1000-10000 on request
HTK 400 GR/22-1G Graphite 2500 x 2300 x 2600 3800
400 650 x 700 x 900 630 x 680 x 900
2200 2200 ± 10 10 12
250 400 (3P) 3 x 370 3 x 500
5x10-3 rough or fine vacuum
200 23
1000-10000 on request
HTK 600 GR/22-1G Graphite 2500 x 2500 x 2900 4500
600 650 x 750 x 1200 630 x 730 x 1200
2200 2200 ± 10 10 12-16
300 400 (3P) 3 x 450 3 x 500
5x10-3 rough or fine vacuum
2200 23
1000-10000 on request

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